How to Learn to Operate a Infinity Supercritical 10L CO2 Extractor

Start First Extraction Using Hops With Known Oil Content

The best way to learn a supercritical CO2 extraction is to first get system training. This can be done at our shop in Ferndale, WA, or with our certified factory rep in Long Beach, California.

You should practice with your 10L system within 1 week of training, or you most likely will forget what you learned. Practice = experience.

The first practice runs should be with CO2 only, and running the system to pressure without any botanicals.

Then do a minimum of 10 runs with leaf beer hops. Order beer hops with known oil content (8-20 percent works great). This will give you valuable experience in starting and running the machine. Make a deal with your local hops supplier to do extracts for them in exchange for the hops if you want. Otherwise, just purchase the hops.

The common question we get from customers: But we already have cheap trim ! Do you know the oil content of the trim? No. But it’s free.  Well, how do you know if it has any oil in it ? Um, we don’t. So how much oil can you extract from that cheap trim with unknown oil quantity ? We don’t know, but nothing is coming out.

If you want to be a successful extractor, please follow our guidance.

Hops Suppliers:

Washington State (our supplier):

Email: Robert Northcorner <north.corner.brewing@gmail.com>

TEL:  (360) 714-1186

Website: http://www.northcornerbrewing.com

Here are the 3 least expensive options:  oil content expressed in

ML/100g, all 1# packaged units

Cascade:  $12.79/#  .8-1.5  (8-15 percent)

Willamette: $13.80/#  1-1.5 (10-15 percent)

Millennium:  $14.69/#  1.8-2.2  (18-22 percent)

In the Los Angeles Area (California):

Eagle Rock Brewing Supply

Email: EagleRockHBS@yahoo.com

TEL: (323) 258-2107

Website: http://www.eaglerockhomebrewing.com

4981 Eagle Rock Blvd

Los Angeles, CA 90041

Culver City Home Brewing Supply

Email: CCHBS@yahoo.com

TEL: (310)397-3453

4234 Sepulveda Blvd

Culver City, CA 90230

South Bay Brewing Supply

Email: brew@southbaybrewing.com

TEL: (310) 328-2133

Website: http://www.southbaybrewingsupply.com

1311 Post Ave

Torrance, CA 90501

 

 

Test Your Botanicals For Oil Content

Get your trim or botanicals tested. It’s the only way to determine how much oil you can extract. If you have cheap or free trim, you may not have any oil content for extracting.

Testing is inexpensive, and a good insurance policy that you are buying what is advertised. If you get free trim, that is not tested, don’t expect any results.

Cannabis Testing and Potency Services

California (here are some options – or google “Los Angeles cannabis testing”:

Coastal Analytical

Email:  info@coastalanalytical.com

TEL: (442) 222- TEST

Website: https://coastalanalytical.com

300 Carlsbad Village Drive

Suite 108A-415

Carlsbad, CA 92008

Pure Analytics

Email: info@pureanalytics.net

TEL:  (888) 505-7108

Website: http://pureanalytics.net

SC Labs

Email: info@sclabs.com

TEL: (866) 435-0709

Website: https://www.sclabs.com

PharmLabs

Email: INFO@PHARMLABSCANNABISTESTING.COM

TEL: (619) 356-0898

Website: https://www.pharmlabscannabistesting.com

Botanical Oil Extraction War of the Solvents

Which solvent is best ? Research and you decide.

BHO and Ethanol Solvent

 Hydrocarbons (such as Butane or BHO) and Ethanol are cheap solvents, that can degrade terpenes, nutraceuticals, and extract non-desirable components that require a great deal more post-processing. Both are highly flammable and explosive. So much, that specially designed blast rooms are required for code, and are outlawed in some areas. BHO specifically, can leave residues, which if are not properly removed during distillation, can result in nose-burn or heart aches (Google – butane in the bloodstream or dangers of butaneingestion for more info). If not properly processed, BHO only has a shelf-life of a few weeks. Reference: Human Toxicity of Butane

 CO2 Solvent

 CO2 is one of the preferred solvents for botanical extraction, which can better target oil (minimize wax and other undesirable extractions which need to be post-processed removed). It has a relatively unlimited shelf life if properly prepared. With proper extraction technique, CO2 can preserve both terpenes and nutraceuticals.

Organic Extraction Using Water

Using water as the botanical oil extraction method is the holy-grail of methods, since it does not require high-pressure gas containment, and uses one of the most abundant elements available, water.

 An additional benefit is that it is a organic process, can be continuous feed, and smaller footprint with less overall equipment costs in large processing operations. 

Currently there is only one manufacturer that builds the SDR (Spinning Disc Reactor) for this method of botanical oil extraction, Infinity Supercritical.

 

Terpenes | Fractionation | Supercritical CO2 Extraction

http://www.infinitysupercritical.com

Email: greg@infinitysupercritical.com

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Supercritical CO2 | Cannabis | CBD | Cannabidiol | Cannabinoids

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Winterizing | Post Processing

infinity-supercritical-co2-hops-extraction-flow-bar-2
Supercritical CO2 Extract

Post Processing Options:

http://www.infinitysupercritical.com/post-processing-equipment.html

We have a new de-waxing machine, and we are working on a complete winterizing and dewaxing machine.

CO2 Post Processing Details:

In some cases, with proper CO2 extraction technique, the extract (crude) oil can be used directly. For consumer use, you may wish to post-process to purify for concentrates to be used for vape pens, dabs, edibles, and other uses.

1. CO2 Extraction results in extract – which can be called crude oil.
2. Winterization: put crude oil extract into ethanol.
3. – Mix in ethanol
4. – Chill
5. – filter oil through media (paper) filters or we offer a large filter system
6. – 1-4 passes to remove waxes, using finer filters
7. – Rotovape to remove ethanol (evaporation in a rotary vessel and vacuum)
8. – At this point you can put into a vacuum oven and then it is ready for Vape Pens
9. If you want to make your own recipies for custom vape pen or concentrations, you can do distillation: CBN, CBD, and THC. Isolate waste versus desired components. The distillation can be flash chromotography, thin film, or standard distillation system.
10. End product is high THC extract, called a concentrate. That can be used directly in vapes, or cut with coconut oil or PEG for vape pens. One extract has a multitude of end consumer products.

Example of Post Processing Video on YouTube:

https://youtu.be/6aWvP02fqoI

Making Shatter: Shatter needs to have the terpenes (the flavinoid component) removed as much as possible from the oil. Then removal of any small amount of waxes (typically by Winterization). Finally, the product is put into a vacuum oven.

Customer Testimonial – Maine – Medical Marijuana:
The only post processing I do now is use a vacuum oven on a very low temp just to dehydrate the hydrosols.  The end result is a beautiful HTFSE that needs no carrier and can be loaded directly into vape pens for a tasty solvent less extract.

Winterizing and Distillation Equipment Pricing From Infinity Supercritical

If you are just making vape pens, all you need is the winterizing
equipment. If you want to make custom concentrates, so you can control
the percentages of THC and CBD’s, then I recommend both the
Winterizing Equipment and Distillation Equipment.

I have listed a small and medium system equipment options.

Small Processing Lab Equipment: Doing 1-3 runs per day.

Medium to Large Processing Lab Equipment: Above 3 runs per day.

Winterizing Equipment:  (Note: Prices are for example only)
1. Dewaxing Fast Filter (equipment to filter out the wax, after the
botanical crude oil has been mixed with ethanol and put into a freezer
overnight):
Medium: 5L $9,999+
Large: 10L $16,999+
2. Rotary Evaporator (evaporates the ethanol used to mix up the
botanical oil in solution to remove the wax):
Small: 2L with chiller, diaphram pump, and accessories package: $10,000+
Medium 20L with chiller, diaphram pump, and accessories package: $30,000+
3. Vacuum Oven (evaporates any water):
Medium: 1.9 CF: $5,000+

Distillation Equipment (used to heat up concentrated oil and separate
into fractions of THC, CBD, and other compounds if selected):
Small: 5L Short Path Distillation Package with Chiller and
accessories package: $16,000+
Medium: 10L Short Path Distillation Package with Chiller and
accessories package: $30,000+

A small lab set-up is around $50,000 +

A medium lab set-up is around $80,000 +

 

Cannabis Search Engine Series Winterization | Oil Extraction | Post Processing | Supercritical CO2 Fluid Extraction 

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November 16, 2016

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Using Supercritical CO2 Extraction to Make Hops Oil

http://www.infinitysupercritical.com

Email: greg@infinitysupercritical.com

Cannabis Search Engine Series Hops | CO2 Extraction | Oil Separation | Supercritical CO2 Fluid Extraction

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November 16, 2016

PDF Source:  01.pdf |  Hops and Hops Extract

PDF Source:  1.pdf |  Extraction and Fractionation of Natural Organic Compounds from Plant Materials with Supercritical Carbon Dioxide

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Supercritical CO2 Extraction Carry Over – How to prevent CO2 pump clogging

Carry -Over

CO2 changes states at different temps and pressures. This gives us the abilitility to control very specifically what kind of solvent we are using, as well as, overall yield. So it is possible to lower settings to achieve a softer solvent extraction, or higher settings to get a stronger solvent extraction. The extraction process with CO2 makes it possible to control separator settings, that drop-out the extracted oil from the CO2 gas solvent. This can effect carry-over amounts as well as quality of the final product. To limit loss of collection and fractionation of both terpenes, THC, and Cannabinoids, you need to lower the pressure of the CO2 and entrained oil. As the CO2 expands, and drops pressure, a huge amount of temperature drop occurs, which necessitates the use of heat during expansion. For lower CO2 gas pressure, a heat exchanger or chiller can be utilized to lower gas temperatures on the back end of the collection vessels, which lowers the pressure.

There are a number to techniques to help reduce or eliminate carry-over. One innovation that Infinity Supercritical has developed, is using electrostatic precipitation. A small charge is introduced (passively) into the CO2 gas and entrained oil, which charges the oil and makes it stick to the nearest opposite charged surface (collection vessel).

Cannabis oil which is not collected (termed carry-over), will continue through the closed-loop system and can clog the diaphragm pump, or the liquid CO2 pump, which will required down-time and maintenance to change the spring energized seals, and o-ring seals. This is such a problem with many commercial extraction systems, that many operators have complete spare pumps which they can replace, so that the downtime of the processing is kept to a minimum.

Contributors: Clinton S and Infinity Supercritical Staff.

SBR Spinning Ball Rotavap a new advancement in ethanol evaporation from botanical oil extracts

Infinity Supercritical is working on a LEEP technology for the evaporation of ethanol from a oil liquid. LEEP stands for Liquid Evaporation by Electrostatic Precipitation, and is a new innovation in the rotary evaporation field.

The new technology may provide the following benefits compared to legacy evaporation of ethanol using a rotary evaporation system:

  • Less cleaning
  • Better user experience
  • Faster evaporation and collection of ethanol (for recycled use)
  • Does not require the use of a vacuum pump (although one may be used)
  • Rapid heat transfer in both the evaporation and condensation end of the process
  • Straight walled Borosilicate glass can be cleaned with a spatula
  • No complex glass work, breakage, or cleaning
  • Larger volumes of processed liquid in a smaller space
  • Less parts = less maintenance = lower acquisition cost
  • Glasswork is stationary, it does not move
  • Solid state rotary evaporation process
  • Uses electrostatics to manipulate boundary layer and surface tension
  • Elimination of vapor layer increases heat dissipation capacity up to 45x

For more information, please contact Infinity Supercritical.

Infinity Electrostatics Announces New Technology for Tracking Materials – The Blockchain Crypto Carbon Fingerprint

PDF: 20171227-infinity-electrostatics-crypto-carbon

Infinity Electrostatics LLC, a technology development firm for additive 3D printing and graphene production, is pleased to announce development of a unique process to track materials.

Using graphene (produced from graphite, or eco-friendly hemp and bamboo), almost any carbon-based material can be used to make a identifiable carbon fingerprint.

What do you get when you combine a strand of carbon atoms, RFID, barcode, born-on-date, and location in one structure ? You get a thread that resembles a DNA of data. Since each thread is unique, it may be used in different products, but it’s origin and identifier will always be the same. This allows your unique product to be distributed, but not copied, without its fingerprint.

The crypto carbon blockchain technology gives you a competitive advantage in the market, by having a market identifiable history from inception. It is the new crypto carbon of industry. In a distributed material chain, it provides a mechanism of accountability using a carbon DNA fingerprint which can’t be erased.

20171224-infinity-electrostatics-graphene-energy-tube-05
Carbon based material matrix, such as carbon fiber can be made from crypto carbon thread.

Using this material in consumer products from clothes to phones, can allow sensors to determine and quantify data of origin (real versus knock-offs), use, and consumer metrics. When a crypto carbon sensor is connected to a network, it can give real-time channel specific traffic data to the factory on product robustness, and tampering.

Since the crypto carbon is invisible to the eye, it provides a transparent barcode. Carbon based graphene is also conductive, so it can also be used as a RFID (radio frequency identification). Since crypto carbon can be statically charged, a RFID can be self-powered.

About Graphene:  The new environmentally friendly, transparent, go-to material that has incredible opportunities for super capacitors, solar cells, semi-conductors, is impervious to water, temperature changes, and can self-repair its bonds. It is 1000 times more conductive than Copper, 200 times stronger than steel, and doesn’t have the limitations of silicon.

20171227-infinity-electrostatics-crypto-carbon

Infinity Electrostatics Announces New Technology for Producing Graphene

PALO ALTO, Calif., Dec. 21, 2017 (GLOBE NEWSWIRE) — Infinity Electrostatics LLC, a technology development firm for additive 3D printing, is pleased to announce a new method of production for graphene.

Graphene is the new environmentally friendly, transparent, go-to material that has incredible opportunities for super capacitors, solar cells, semi-conductors, is impervious to water, temperature changes, and can self-repair its bonds. It is 1000 times more conductive than Copper, 200 times stronger than steel, and doesn’t have the limitations of Silicon.

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Graphene can be used in bioengineering, optics, composites, energy storage, photovoltaics, and even as ultrafiltration, as a thin membrane for seawater desalination. It can be laser printed. Using quantum dots, band gaps can be generated to utilize in the semiconductor industry.

The limitation of graphene development and use in industry, is its production. Infinity has developed a method, using a Spinning Disc Reactor, to provide a low cost method of producing graphene, using sonification and shearing.

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Infinity Electrostatics LLC develops and markets innovative additive 3D printing technology. Emphasis is placed on developing new technology to reduce additive build time, and producing a superior 3D printed product, maximizing efficiency of powder distribution, and reducing additive layer binding time. Industries served include laser engraver and fiber cutting machine manufacturers, additive 3D metal printing, and electrostatics. Please visit http://www.infinityelectrostatics.com for more information.

 

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