Terpenes | Initial Cold Run | Consulting

What Are Terpenes ?

Terpenes are found in the essential oils of plants. The aeromatic nature of the Terpene give Cannabis its unique smell.

Terpenes rentention throughout the entire process is critical. The colder you can maintain your extractor will help with a beautiful final wax. It is important to remember you are working soft plant matter, It doesnt take a hammer to smash a bannana. If would like to
get the best insider training straight from Southern Oregons emerald triangle in co2 extraction all the way to a final product dispensary, I have built a successful co2 company from the ground up, including experience in rotovap, vac oven,winterazation, and
most importantly, simple water removal from wax (this can ruin a whole batch).

Contact Clinton S:
blue.pool.llc@gmail.com

What Are Terpenes ?

What are Terpenes ?
Terpenes are found in the essential oils (flavinoids) of plants,
consisting of a large group of volatile unsaturated hydrocarbons.
Found commonly in conifers and citrus trees. In Cannabis,
terpenes are the oily compound, and the main building block
of resin that contribute to the flavor, scent and color of the oil.
The aeromatic nature of the Terpene give Cannabis its
unique smell. Terpenes are volatile molecules that evaporate
easily, and are oily compounds secreted by the plants
Trichomes. Cannabinoids and Terpenoids develop from THC
and Terpenes that infuse the plants flower tops,
share the same biochemical precursor (Geranyl
Pyrophosphate). Terpenes have the aroma, while Cannabinoids
are odorless.

In extraction, Terpenes can be extracted separately than the
Cannabinoids, and recombined at the end of the extraction
process. Terpenes are generally extracted in lower pressure
and no heat.

What about Terpenes during Decarboxylation ?
“ Besides cannabinoids, the cannabis plant contains a range of terpenes, which are the volatile compounds that give cannabis its distinct smell and may act synergistically with cannabinoids. Although preheating the plant material may release more of the known active (neutral) cannabinoids, it may simultaneously also cause loss by degradation or evaporation of components such as terpenes. Our tests were intended to better clarify the balance between desired decarboxylation and unwanted degradation. Unheated cannabis material was analyzed as a control.”
Source: Cannabis Oil: chemical evaluation of an upcoming cannabis-based medicine
Luigi L Romano, Arno Hazekamp
Department of Pharmacy, University of Siena, Italy
Plant Metabolomics group, Institute of Biology, Leiden University, The Netherlands

Cannabis Cannabinoids, Terpenes and Flavonoids

Phytocannabinoids

THC (Δ-9-tetrahydrocannabinol)
Boiling point: 157° C / 314.6° Fahrenheit
Properties: Euphoriant, Analgesic, Anti Inflammatory, Antioxidant, Antiemetic

CBD (cannabidiol)
Boiling point: 160-180°C / 320-356° Fahrenheit
Properties: Anxiolytic, Analgesic, Antipsychotic, Anti Inflammatory, Antioxidant, Antispasmodic

CBN (Cannabinol)
Boiling point: 185°C / 365° Fahrenheit
Properties: Oxidation, breakdown, product, Sedative, Antibiotic

CBC (cannabichromene)
Boiling point: 220° / 428° Fahrenheit
Properties: Anti Inflammatory, Antibiotic, Antifungal

Δ-8-THC (Δ-8-tetrahydrocannabinol)
Boiling point: 175-178°C / 347-352.4° Fahrenheit
Properties: Resembles Δ-9-THC, Less psychoactive, More stable Antiemetic

THCV (Tetrahydrocannabivarin)
Boiling point: < 220°C / <428° Fahrenheit
Properties: Analgesic, Euphoriant

Terpenoid Essential Oil Components of Cannabis

β-Myrcene
Boiling point: 166-168°C / 330.8-334.4° Fahrenheit
Properties: Analgesic. Anti Inflammatory, Antibiotic, Antimutagenic

β-Caryophyllene
Boiling point: 119°C / 246.2° Fahrenheit
Properties: Anti Inflammatory, Cytoprotective (gastric mucosa), Antimalarial

d-Limonene
Boiling point: 177°C / 350.6° Fahrenheit
Properties: Cannabinoid agonist?, Immune potentiator, Antidepressant, Antimutagenic

Linalool
Boiling point: 198°C / 388.4° Fahrenheit
Properties: Sedative, Antidepressant, Anxiolytic, Immune potentiator

Pulegone
Boiling point: 224°C / 435.2° Fahrenheit
Properties: Memory booster?, AChE inhibitor, Sedative, Antipyretic

1,8-Cineole (Eucalyptol)
Boiling point: 176°C / 348.8° Fahrenheit
Properties: AChE inhibitor, Increases cerebral, blood flow, Stimulant, Antibiotic, Antiviral, Anti Inflammatory, Antinociceptive

α-Pinene
Boiling point: 156°C / 312.8° Fahrenheit
Properties: Anti Inflammatory, Bronchodilator, Stimulant, Antibiotic, Antineoplastic, AChE inhibitor

α-Terpineol
Boiling point: 217-218°C / 422.6-424.4° Fahrenheit
Properties: Sedative, Antibiotic, AChE inhibitor, Antioxidant, Antimalarial

Terpineol-4-ol
Boiling point: 209°C / 408.2° Fahrenheit
Properties: AChE inhibitor. Antibiotic

p-Cymene
Boiling point: 177°C / 350.6° Fahrenheit
Properties: Antibiotic, Anticandidal, AChE inhibitor

Borneol
Boiling point: 210°C / 410° Fahrenheit
Properties: Antibiotic

Δ-3-Carene
Boiling point: 168*C / 334.4° Fahrenheit
Properties: Anti Inflammatory

Flavonoid and Phytosterol Components of Cannabis

Apigenin
Boiling point: 178°C / 352.4° Fahrenheit
Properties: Anxiolytic, Anti Inflammatory, Estrogenic

Quercetin
Boiling point: 250°C / 482° Fahrenheit
Properties: Antioxidant, Antimutagenic, Antiviral, Antineoplastic

Cannflavin A
Boiling point: 182°C / 359.6° Fahrenheit
Properties: COX inhibitor, LO inhibitor

β-Sitosterol
Boiling point: 134°C / 273.2° Fahrenheit
Properties: Anti Inflammatory, 5-α-reductase, inhibitor

What Is Decarboxylation ?

What is Decarboxylation, and why do I need to convert THCA to THC ? 

Decarboxylation (or decarbing) is removing the CO2 and water vapor (COOH) from the botanicals, which can be done in an oven, or over time via air drying. It’s a chemical reaction which carboxylic acids loose a carbon atom in the carbon chain, that converts THCA to THC. 30 minutes at 240 F or 115 C. The results are dramatic. With a 30 minute decarb, THC in Kief can go from 3.8 percent to 25.4 percent. The THCA with 30 minutes goes from 24.5 percent to 2.6 percent. Longer times did not result in any statistically better percentages, but no more than 60 minutes is required. For Cannabis Trim, the THC goes from .6 percent to 4.8 percent, while the THCA goes from 6.5 percent to 2.9 percent. Again, a longer decarb did not result in much better percentages, however depending on moisture content, times do not need to exceed 60 minutes. However, decarbing might reduce or destroy Terpenes (see below). A combined Terpene extraction, followed by decarb, and then extraction may be worth trying. Moisture content will effect time in the oven. More moisture = more time.

img_7392
Properly Decarboxylating Cannabis Provides More THC

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PDF Source:  AspUserGuide10.pdf |  Aspen Plus User Guide

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PDF Source:  CO68.pdf |  SUPERCRITICAL FLUID EXTRACTION OF CANNABIS: EXPERIMENTS AND MODELING OF THE PROCESS DESIGN

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PDF Source:  1d_Extracts_and_Infusions.pdf |  Methods for Producing and Testing Extracts and Infusions 

PDF Source:  2014-11-06-cannabis 201-slides.pdf |  Cannabis Chemistry 201

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PDF Source:  1d_Extracts_and_Infusions.pdf |  Methods for Producing and Testing Extracts and Infusions 

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PDF Source:  MatMed5.pdf |  HERBAL MATERIA MEDICA

PDF Source:  MCC-Patient-Education-Handbook.pdf |  PATIENT EDUCATION HANDBOOK Cannabis

PDF Source:  MED_Equivalency_Final 08102015.pdf |  Marijuana Equivalency in Portion and Dosage

PDF Source:  medical-marijuana-for-non-smokers_compassioncenter.net.pdf |  Medical Marijuana for Non-Smoking Older Patients

PDF Source:  Medical_Marijuana_Patient_Handbook_Mass.pdf |  MASSACHUSETTS MEDICAL MARIJUANA PATIENT HANDBOOK 

PDF Source:  MedicalBooklet-V6.pdf |  HOW TO MAKE MEDICINAL CANNABIS PREPARATIONS

PDF Source:  NORML_Clinical_Applications_for_Cannabis_and_Cannabinoids.pdf |  Emerging Clinical Applications for Cannabis and Cannabinoids

PDF Source:  P06.pdf |  Supercritical CO2 extraction of oregano and clove buds mixture-synergistic effect and chemical composition of extract

PDF Source:  Russo et al. Cannabis Night Vision JEP 2004.pdf |  Cannabis improves night vision: a case study of dark adaptometry and scotopic sensitivity in kif smokers of the Rif mountains of northern Morocco

PDF Source:  Salve.pdf |  Cannabis Processing for THC, CBD & Terpenes Initiated 5/2/14

PDF Source:  sawpalmetto.pdf |  Saw Palmetto

PDF Source:  Science Cannabis.pdf |  The Science of Marijuana

PDF Source:  The_World_of_Concentrates.pdf |  The World of Cannabis Concentrates

PDF Source:  TheBreeding_Varieties.pdf |  The Breeding and Parentage of Hop Varieties

PDF Source:  UCF-Arboretum-Herbal-Guide1.pdf |  UCF Arboretum’s Herbal Guide A health guide of medicinal herbs, culinary herbs, and super foods

PDF Source:  vegetable glycerin cannabis tincture.pdf |  VEGETABLE GLYCERIN CANNABIS TINCTURE

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November 16, 2016

PDF Source:  01-001CH 274 Hemp Rules.pdf |  Rules for Growing Industrial Hemp

PDF Source:  0714-164054-5102-02 Cannabinoids in Marijuana and Edibles by QuEChERS.pdf |  Extraction of Cannabinoids in Marijuana and Edibles by QuEChERS

PDF Source:  09.pdf |  Marijuana and the Cannabinoids ElSohly

PDF Source:  1030ae0323a3140ecf531bd473632b57.pdf |  Illegally green: environmental Costs of Hemp Prohibition

PDF Source:  13-06-European-Hemp-Industry.pdf |  The European Hemp Industry Cultivation, processing and applications for fibres, shivs and seeds

PDF Source:  153-830-1.pdf |  Industrial Hemp Enterprise

PDF Source:  25.pdf |  Overview of the history of Cannabis Hemp

PDF Source:  42z4250f54vbjd.pdf |  MGC License Approvals Set to Fast Track Commercialisation

PDF Source:  647867.pdf |  Design of Competitive Processing Plants for Hemp Fibre Production

PDF Source:  720005287en.pdf |  Purification of Cannabidiol from Hemp Oil Using the Prep 150 LC System

PDF Source:  ages001e_1_.pdf |  Industrial Hemp in the United States: Status and Market Potential

PDF Source:  ages001ei_1_.pdf |  Hemp Potential US Production and Processing

PDF Source:  AJPS_2015010611240521.pdf |  Evaluation of Protein Concentration, Amino Acid Profile and Antinutritional Compounds in Hempseed Meal from Dioecious and Monoecious Varieties

PDF Source:  All-About-Hemp-Plant-HempInc-eBook.pdf |  ALL ABOUT THE HEMP PLANT 10,000 Years of History

PDF Source:  australia16.pdf |  New Tropical Industrial Hemp

PDF Source:  Bergamaschi_2011.pdf |  Safety and Side Effects of Cannabidiol, a Cannabis sativa Constituent

PDF Source:  brochure.pdf |  Industrial Hemp

PDF Source:  cannabis-extract-report.pdf |  Cannabis Extracts to Treat Diseases

PDF Source:  cannabis_cultivation17_ultimate.pdf |  Cannabis Indoor Cultivation Usage Guide

PDF Source:  cannabis_graphene.pdf |  Interconnected Carbon Nanosheets Derived from Hemp for Ultrafast Supercapacitors with High Energy

PDF Source:  CBD-Reintroduction-Era-2011.pdf |  As CBD-Rich Cannabis Strains Proliferate, Clinicians Develop Survey to Document Effects 

PDF Source:  cs_apca.pdf |  INDIAN HEMP Apocynum cannabinum L

PDF Source:  Dixie-one-page.pdf |  Medical Marijuana, Inc Pitching CBD Products

PDF Source:  DrRima.CBD_.Dossier.pdf |  Natural Solutions Corporation Chile SpA

PDF Source:  Ecological-benefits-of-hemp-and-flax-cultivation-and-products-2011.pdf |  Ecological benefits of hemp and flax cultivation and products

PDF Source:  en_2013_01_1.pdf |  Cannabis Oil: chemical evaluation of an upcoming cannabis-based medicine

PDF Source:  eric_steenstra.pdf |  Legalizing Industrial Hemp in the States

PDF Source:  GuidelinesForGrowingHemp.pdf |  Guidelines for growing Hemp

PDF Source:  HB2238P.pdf |  HCS HB 2238 – CBD OIL

PDF Source:  Hemp-Facts-from-Drug-War-Facts.pdf |  Hemp Facts from Drug War Facts

PDF Source:  hemp-toolokit.pdf |  Hemp

PDF Source:  hemp.pdf |  Industrial Hemp and its Potential for New Zealand

PDF Source:  hemp97.pdf |  INDUSTRIAL HEMP: GLOBAL MARKETS AND PRICES

PDF Source:  hemp_crop_description.pdf |  Industrial Hemp Production Basics

PDF Source:  hemp_for_headache.pdf |  Hemp for Headache: An In-Depth Historical and Scientific Review of Cannabis in Migraine Treatment

PDF Source:  HEMP_Processor.List.pdf |  Kentucky Department of Agriculture Industrial Hemp Pilot Program

PDF Source:  hempproduction.pdf |  Industrial Hemp Production

PDF Source:  HHO-PDF-IsCBDLegal.pdf |  Is Cannabidiol CBD Oil Legal What About for Your Country

PDF Source:  HIA-position-CBD-FINAL.pdf |  Hemp Industries Association Position on CBD Extracts Misbranded and Marketed as Hemp Oil

PDF Source:  industrialhemp.pdf |  Hemp

PDF Source:  KerrIHbenefits.pdf |  The Environmental Benefits of Using Industrial Hemp

PDF Source:  Latvia_ESRD_37_2015-105-113.pdf |  RISK ASSESSMENT IN HEMP (Cannabis sativa L.) PRODUCTION AND PROCESSING

PDF Source:  nrcs142p2_053283.pdf |  Sunn Hemp: A Cover Crop for Southern and Tropical Farming Systems

PDF Source:  PRODUCT-CATALOG-PDF_BUYCBDpg.pdf |  Hemp Derived CBD Oil

PDF Source:  projectcbd_special-report_medical-marijuana-inc-hempmeds-kannaway.pdf |  HEMP OIL HUSTLERS A Project CBD Special Report on Medical Marijuana Inc.

PDF Source:  RL32725-20140214.pdf |  Hemp as an Agricultural Commodity

PDF Source:  RL32725.pdf |  Hemp as an Agricultural Commodity

PDF Source:  Rosenfeld.pdf |  Responsible Phytocannabinoid Therapies

PDF Source:  Rymkenafhemp.pdf |  Kenaf and Hemp Identifying the Differences

PDF Source:  S0990.pdf |  RELATING TO AGRICULTURE AND FORESTRY – CBD-RICH HEMP ACT

PDF Source:  SEI-Report-EcologicalFootprintAndWaterAnalysisOfCottonHempAndPolyester-2005.pdf |  Ecological Footprint and Water Analysis of Cotton, Hemp and Polyester

PDF Source:  small.pdf |  Hemp: A New Crop with New Uses for North America

PDF Source:  ST-NAR-40-Ebook.pdf |  Recommended methods for the identification and analysis of cannabis and cannabis products

PDF Source:  stpap443.pdf |  Is Industrial Hemp Worth Further Study in the U.S.? A Survey of the Literature

PDF Source:  uk_hempproduction_2013.pdf |  Industrial Hemp Production

PDF Source:  vol23p555.pdf |  THE LEGALIZATION OF INDUSTRIAL HEMP AND WHAT IT COULD MEAN FOR INDIANA’S BIOFUEL INDUSTRY

PDF Source:  W328.pdf |  STATUS OF INDUSTRIAL HEMP PRODUCTION IN TENNESSEE IN 2015

PDF Source:  WP2014-10.pdf |  Industrial Hemp: Opportunities and Challenges for Washington